Adhesion and interfacial characterization of biomimetically texturized lithium disilicate

Lithium disilicate glass-ceramic (LS2) can be biomimetically textured by crystal orientation, mimicking the microstructure of dental enamel and inducing anisotropic mechanical responses to crack growth. The deliberate texturization of LS2 plays to the clinical advantage of reinforcing weak sites of typical fracture initiation in dental prosthetic constructs. Similar to enamel, adhesion of biomimetically textured LS2 could also show anisotropic behavior. Therefore, tensile bond strength (TBS) before and after thermocycling (TC) and interfacial characterization of biomimetically textured LS2 (parallel (PAR) or perpendicular (PER) crystal orientation) after different pre-treatment modes (hydrofluoric acid etching (HFE), grit blasting (GBL) and self-etching glass-ceramic primer (SGP)) were investigated. TC reduced significantly TBS for all specimens except for GBL. Biomimetic textured LS2 after HFE showed anisotropic behavior regarding adhesion. Crystal orientation reduced TBS for the PER HFE specimens after TC significantly. In general, the TBS of HFE specimens was still higher or not significantly lower compared to other pre-treatment modes like GBL or SGP. For the GBL and SGP specimens, crystal orientation had no influence on TBS and interfacial characteristics. In contrast HFE specimens showed different interfacial characteristics depending if they were PAR or PER texturized. Based on these findings, HFE of biomimetic textured LS2 can be recommended. For bonding, the PAR orientation is recommended as its adhesion potential is less prone to degrade.     

Development of mullite fibers and novel zirconia-toughened mullite fibers for high temperature applications

Polycrystalline mullite fibers and novel zirconia-toughened mullite (ZTM) fibers with average diameters between 9.7 and 10.3 μm containing 3, 7 and 15 wt.-% tetragonal ZrO₂ (ZTM3, ZTM7, ZTM15) in the final ceramic were prepared via dry spinning followed by continuous calcination and sintering in air. A shift in the formation of transient alumina phases and tetragonal ZrO₂ to higher temperatures with increasing amounts of ZrO₂ was observed. Concomitantly, the mullite formation temperature was lowered to 1229 °C for ZTM15 fibers. X-ray diffraction revealed formation of the desired tetragonal crystal structure of ZrO₂ directly from the amorphous precursor. Room temperature Weibull strengths of 1320, 1390 and 1740 MPa and Weibull moduli of 9.5, 7.1 and 9.0 were determined for mullite, ZTM3 and ZTM15 fibers, respectively. Average Young’s moduli ranged from 190 to 220 GPa. SEM images revealed crack-free fiber surfaces and compact microstructures independent of the amount of ZrO₂.     

Predicting the tensile creep of concrete

Over a four year period, six phases of testing were performed to observe the influence of age at loading, applied stress level, mix composition and relative humidity on the tensile creep of concrete. From these investigations it was possible to develop a model which allowed the prediction of tensile creep based on a knowledge of the compressive strength of the concrete (determined at the age of loading), the applied stress level and the relative humidity. Subsequently, this model was validated using the results from three independent investigations. Compressive creep as well as tensile creep was also obtained. This allowed a comparison of compressive creep with tensile creep and illustrated that on the basis of equal stresses, tensile creep is on average between 2 and 3 times greater than compressive creep (the maximum ratio is in excess of 8). For this investigation, however, on the basis of stress/strength ratio the difference between tensile and compressive creep is less significant. Considering a simply supported flexural reinforced concrete element, the investigation suggests that it is unwise to consider actual compressive creep equal to actual tensile creep as is often the case in design practice.     

A Generalized Relationship for Determination of Tensile Strength of Fine-Grained Soils from Shrinkage Characteristics

Tensile strength of fine-grained soils has been extensively investigated by earlier researchers and several methodologies have been evolved for its determination. However, either most of these methods are not valid/applicable for a wide range of moisture contents or they involve tedious sample/specimen preparation. In this context, the methodology of determining tensile strength by employing thin films, which is available in the literature, has been found to be quite handy and useful. It has been observed that a unique relationship exists among the tensile strength, moisture content, and shrinkage characteristics of fine-grained soils. This methodology is appreciable due to its applicability to a wide range of moisture contents, comparable ease of sample preparation and testing, and the obtained results lack generalization. Exhaustive tests were conducted on fine-grained soils of entirely different characteristics and generalized relationships have been proposed between the percentage linear shrinkage, tensile strength, and moisture content (defined as liquid to solid ratio). Based on a critical analysis of the results available in the literature, the efficiency of such relationships for determination of tensile strength of fine-grained soils has been demonstrated. In the authors’ opinion, such relationships would be quite useful for determining tensile strength of fine-grained soils from their linear shrinkage, which can easily be measured in a conventional geotechnical engineering laboratory.     

Evaluation of Tensile and Fatigue Properties of Metals Using Small Specimens

Small specimens are increasingly being used in getting mechanical properties directly when there are limited materials to facilitate standard specimens, which play a great role in the rapid measurement of mechanical properties and residual life assessment of in-service reactor components. Although tensile and fatigue properties of the small specimens are investigated extensively, theoretical models for describing the mechanical properties of small specimens need to be established. Here, we conduct a systematic investigation of tensile and fatigue properties of pure Cu specimens with thicknesses ranging from 3 to 0.2 mm. The results show that the decrease in uniform elongation of the 0.2 mm-thick specimens is mainly due to the effects of grain boundary and free surface on the strain hardening rate. A modified theoretical model correlated with the ratio of the surface grain layer thickness to the grain size is proposed to predict variation in yield strength of the small specimens more accurately. Furthermore, the mechanism for the difference in fatigue life between the 0.2 mm-thick specimen and other thicker specimens is elucidated. The Basquin equation-based model is presented as a potential way to evaluate the fatigue life of metals using small specimens.     

Required strength of geosynthetics in a reinforced slope with tensile strength cut-off subjected to seepage effects

The Mohr-Coulomb (M-C) yield criterion is found to overestimate the tensile strength of cohesive soils. By introducing the concept of tensile strength cut-off, the M-C criterion is modified to reduce or eliminate the tensile strength from the criterion. In this study, a new approach is proposed to investigate the stability of geosynthetic-reinforced slopes in cohesive soils subjected to seepage effects by means of the kinematic approach of limit analysis. The distribution of pore-water pressure is obtained using the numerical modeling software package, FLAC3D. A kinematically admissible failure mechanism is discretized to incorporate the results from the numerical simulation. The strength of geosynthetics required for maintaining the slope stability is evaluated from the work-energy balance equation. An optimization routine is used to seek out the maximum value among all possible results. Design charts providing the normalized required reinforcement under different parameters are plotted for a parametric study and convenient use in engineering. The obtained results show that less reinforcement is required in the presence of soil cohesion, and that the inclusion of the effect of tensile strength cut-off leads to a more conservative solution, which is more obvious in the presence of seepage effects.     

A methodology to determine the elastic properties of anisotropic rocks from a single uniaxial compression test

This paper introduces a new methodology to measure the elastic constants of transversely isotropic rocks from a single uniaxial compression test. We first give the mathematical proof that a uniaxial compression test provides only four independent strain equations. As a result, the exact determination of all five independent elastic constants from only one test is not possible. An approximate determination of the Young's moduli and the Poisson's ratios is however practical and efficient when adding the Saint–Venant relation as the fifth equation. Explicit formulae are then developed to calculate both secant and tangent definitions of the five elastic constants from a minimum of four strain measurements. The results of this new methodology applied on three granitic samples demonstrate a significant stress-induced nonlinear behavior, where the tangent moduli increase by a factor of three to four when the rock is loaded up to 20 MPa. The static elastic constants obtained from the uniaxial compression test are also found to be significantly smaller than the dynamic ones obtained from the ultrasonic measurements.     

The Hoek–Brown failure criterion and GSI – 2018 edition

The Hoek–Brown criterion was introduced in 1980 to provide input for the design of underground excavations in rock. The criterion now incorporates both intact rock and discontinuities, such as joints, characterized by the geological strength index (GSI), into a system designed to estimate the mechanical behaviour of typical rock masses encountered in tunnels, slopes and foundations. The strength and deformation properties of intact rock, derived from laboratory tests, are reduced based on the properties of discontinuities in the rock mass. The nonlinear Hoek–Brown criterion for rock masses is widely accepted and has been applied in many projects around the world. While, in general, it has been found to provide satisfactory estimates, there are several questions on the limits of its applicability and on the inaccuracies related to the quality of the input data. This paper introduces relatively few fundamental changes, but it does discuss many of the issues of utilization and presents case histories to demonstrate practical applications of the criterion and the GSI system.     

体外预应力空间张弦梁结构的ANSYS仿真

运用 ANSYS 有限元分析软件对体外预应力空间张弦梁结构模型试验过程进行仿真计算,模拟了结构在张拉状态下的试验过程,分析了结构在张拉施工阶段的受力性能和变形特点,并探讨了不同预应力索间的相互影响。     

轻集料对高强次轻混凝土物理力学性能的影响

研究了轻集料种类及其在粗集料中所占比例、轻集料粒径与级配以及体积砂率对高强次轻混凝土的表观密度、抗压强度、抗拉强度和弹性模量的影响.试验结果表明,轻集料的种类及其在粗集料中所占比例对不同强度等级的高强次轻混凝土具有相似的影响规律,即当轻集料在粗集料中比例不超过50%时,混凝土的抗压、抗拉强度和弹性模量随轻集料掺量变化的变化并不明显,而超过50%时,则随着轻集料掺量增大而明显降低;高强次轻混凝土的力学性能随轻集料粒径减小而提高,间断级配对混凝土的力学性能影响不利;体积砂率存在最佳范围,约为40%左右.